Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001578.D Acq On : 10 May 2018 02:00 Operator : JC/MD Sample : J2649-01 Misc : 5.42g/5mL/100ul/5mL/MSVOA_X/MEOH ALS Vial : 28 Sample Multiplier: 1 Quant Time: May 10 10:53:54 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 231972 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 313602 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 290609 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 171673 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 150876 45.25 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.50% 35) Dibromofluoromethane 5.51 113 114876 41.18 ug/l 0.00 Spiked Amount 50.000 Recovery = 82.36% 50) Toluene-d8 8.72 98 435408 42.76 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.52% 62) 4-Bromofluorobenzene 11.15 95 155462 39.77 ug/l 0.00 Spiked Amount 50.000 Recovery = 79.54% Target Compounds Qvalue 16) Acetone 2.49 43 14944 9.87 ug/l 92 21) trans-1,2-Dichloroethene 3.15 96 2634 0.92 ug/l 91 44) Trichloroethene 7.21 130 50344 14.14 ug/l 100 64) Tetrachloroethene 9.34 164 5571220 1375.38 ug/l 96 93) 1,2,4-Trichlorobenzene 13.65 180 5016 1.09 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed