Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\Data\VX050918\ Data File : VX001579.D Acq On : 10 May 2018 02:27 Operator : JC/MD Sample : J2649-02 Misc : 6.13g/5mL/100ul/5mL/MSVOA_X/MEOH ALS Vial : 29 Sample Multiplier: 1 Quant Time: May 10 05:26:19 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 235966 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 325751 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 304300 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 183515 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 155512 45.85 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.70% 35) Dibromofluoromethane 5.51 113 117743 40.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 81.28% 50) Toluene-d8 8.72 98 455504 43.07 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.14% 62) 4-Bromofluorobenzene 11.15 95 164576 40.54 ug/l 0.00 Spiked Amount 50.000 Recovery = 81.08% Target Compounds Qvalue 16) Acetone 2.48 43 14481 9.40 ug/l 94 27) cis-1,2-Dichloroethene 4.59 96 4760 1.53 ug/l 90 44) Trichloroethene 7.21 130 24648 6.66 ug/l 99 64) Tetrachloroethene 9.35 164 7718024 1819.64 ug/l 95 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed 82X050518W.M Thu May 10 16:35:21 2018