Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001581.D Acq On : 10 May 2018 03:20 Operator : JC/MD Sample : J2649-04 Misc : 4.85g/5mL/100ul/5mL/MSVOA_X/MEOH ALS Vial : 31 Sample Multiplier: 1 Quant Time: May 10 05:32:02 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.66 168 241818 50.00 ug/l -0.01 34) 1,4-Difluorobenzene 6.87 114 334416 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 301861 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 176597 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 163596 47.07 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.14% 35) Dibromofluoromethane 5.51 113 120317 40.45 ug/l 0.00 Spiked Amount 50.000 Recovery = 80.90% 50) Toluene-d8 8.72 98 462995 42.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.28% 62) 4-Bromofluorobenzene 11.15 95 158247 37.97 ug/l 0.00 Spiked Amount 50.000 Recovery = 75.94% Target Compounds Qvalue 64) Tetrachloroethene 9.34 164 9394 2.23 ug/l 90 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed