Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001584.D Acq On : 10 May 2018 04:40 Operator : JC/MD Sample : J2649-07 Misc : 5.96g/5mL/100ul/5mL/MSVOA_X/MEOH ALS Vial : 34 Sample Multiplier: 1 Quant Time: May 10 05:43:01 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 241560 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.86 114 333263 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 303996 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 177357 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 159810 46.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.06% 35) Dibromofluoromethane 5.51 113 119444 40.29 ug/l 0.00 Spiked Amount 50.000 Recovery = 80.58% 50) Toluene-d8 8.72 98 456303 42.17 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.34% 62) 4-Bromofluorobenzene 11.15 95 158925 38.26 ug/l 0.00 Spiked Amount 50.000 Recovery = 76.52% Target Compounds Qvalue 18) Methyl Acetate 2.80 43 53669 12.96 ug/l 99 64) Tetrachloroethene 9.34 164 105948 25.00 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed