Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001586.D Acq On : 10 May 2018 05:34 Operator : JC/MD Sample : J2649-09 Misc : 5.82g/5mL/100ul/5mL/MSVOA_X/MEOH ALS Vial : 36 Sample Multiplier: 1 Quant Time: May 10 08:34:21 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.66 168 244223 50.00 ug/l -0.01 34) 1,4-Difluorobenzene 6.86 114 336769 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 306507 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 178751 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 163201 46.49 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.98% 35) Dibromofluoromethane 5.51 113 120569 40.25 ug/l 0.00 Spiked Amount 50.000 Recovery = 80.50% 50) Toluene-d8 8.72 98 467015 42.71 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.42% 62) 4-Bromofluorobenzene 11.15 95 161968 38.59 ug/l 0.00 Spiked Amount 50.000 Recovery = 77.18% Target Compounds Qvalue 64) Tetrachloroethene 9.34 164 11457 2.68 ug/l 95 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed