Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001589.D Acq On : 10 May 2018 06:53 Operator : JC/MD Sample : J2806-02 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 39 Sample Multiplier: 1 Quant Time: May 10 08:40:29 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 256533 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 346610 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 296456 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 149364 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 170842 46.33 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.66% 35) Dibromofluoromethane 5.51 113 131851 42.77 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.54% 50) Toluene-d8 8.72 98 479111 42.57 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.14% 62) 4-Bromofluorobenzene 11.14 95 143579 33.24 ug/l 0.00 Spiked Amount 50.000 Recovery = 66.48% Target Compounds Qvalue 16) Acetone 2.45 43 3836 2.29 ug/l 94 18) Methyl Acetate 2.79 43 6304 1.43 ug/l 96 20) Methylene Chloride 2.86 84 25247 7.62 ug/l 97 95) Naphthalene 13.84 128 60797 5.49 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed