Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001590.D Acq On : 10 May 2018 07:20 Operator : JC/MD Sample : J2807-04 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 40 Sample Multiplier: 1 Quant Time: May 10 08:42:03 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 274910 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 381191 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 336645 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 184416 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 184495 46.69 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.38% 35) Dibromofluoromethane 5.51 113 141941 41.86 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.72% 50) Toluene-d8 8.72 98 526360 42.53 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.06% 62) 4-Bromofluorobenzene 11.14 95 170391 35.86 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.72% Target Compounds Qvalue 16) Acetone 2.45 43 4173 2.33 ug/l # 81 18) Methyl Acetate 2.78 43 5409 1.15 ug/l 96 95) Naphthalene 13.84 128 22039 1.61 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed