Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001592.D Acq On : 10 May 2018 08:13 Operator : JC/MD Sample : J2807-11 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 42 Sample Multiplier: 1 Quant Time: May 10 12:21:05 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 260833 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 357543 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 314784 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 176210 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 174574 46.57 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.14% 35) Dibromofluoromethane 5.51 113 132985 41.82 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.64% 50) Toluene-d8 8.72 98 491626 42.35 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.70% 62) 4-Bromofluorobenzene 11.14 95 160620 36.04 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.08% Target Compounds Qvalue 68) m/p-Xylenes 10.36 106 3538 0.59 ug/l 98 69) o-Xylene 10.70 106 1408 0.24 ug/l 99 80) 1,3,5-Trimethylbenzene 11.51 105 6428 0.63 ug/l 100 84) 1,2,4-Trimethylbenzene 11.81 105 21483 2.06 ug/l 96 95) Naphthalene 13.84 128 7390 0.57 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed