Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001593.D Acq On : 10 May 2018 08:40 Operator : JC/MD Sample : J2811-03 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 43 Sample Multiplier: 1 Quant Time: May 10 11:31:24 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 262290 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 357322 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 318295 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 176013 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 177203 47.00 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.00% 35) Dibromofluoromethane 5.51 113 138255 43.50 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.00% 50) Toluene-d8 8.72 98 495778 42.73 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.46% 62) 4-Bromofluorobenzene 11.14 95 162363 36.46 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.92% Target Compounds Qvalue 16) Acetone 2.45 43 5313 3.10 ug/l 100 18) Methyl Acetate 2.78 43 6937 1.54 ug/l 99 20) Methylene Chloride 2.86 84 14410 4.25 ug/l 96 44) Trichloroethene 7.22 130 6949 1.71 ug/l 93 68) m/p-Xylenes 10.36 106 6260 1.04 ug/l 97 69) o-Xylene 10.70 106 3287 0.56 ug/l 94 95) Naphthalene 13.84 128 100600 7.72 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed