Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001594.D Acq On : 10 May 2018 09:07 Operator : JC/MD Sample : J2811-06 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 44 Sample Multiplier: 1 Quant Time: May 10 11:36:01 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 263777 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 356501 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 317810 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 173310 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 174510 46.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.06% 35) Dibromofluoromethane 5.51 113 133815 42.20 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.40% 50) Toluene-d8 8.72 98 493183 42.61 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.22% 62) 4-Bromofluorobenzene 11.14 95 163464 36.79 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.58% Target Compounds Qvalue 16) Acetone 2.45 43 7288 4.23 ug/l 98 18) Methyl Acetate 2.78 43 6718 1.49 ug/l 98 20) Methylene Chloride 2.86 84 60691 17.81 ug/l 98 30) Chloroform 5.23 83 1436 0.25 ug/l 97 84) 1,2,4-Trimethylbenzene 11.81 105 2709 0.26 ug/l 99 95) Naphthalene 13.84 128 15479 1.21 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed