Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001598.D Acq On : 10 May 2018 12:11 Operator : JC/MD Sample : VX0510MBL01 Misc : 5.00g/10mL/100uL/5.0mL/MSVOA_X/MEOH ALS Vial : 3 Sample Multiplier: 1 Quant Time: May 11 06:57:05 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 263125 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 358896 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 315957 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 165940 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 224240 59.29 ug/l 0.00 Spiked Amount 50.000 Recovery = 118.58% 35) Dibromofluoromethane 5.51 113 174915 54.79 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.58% 50) Toluene-d8 8.72 98 625963 53.72 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.44% 62) 4-Bromofluorobenzene 11.14 95 202155 45.19 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.38% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed