Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001602.D Acq On : 10 May 2018 15:27 Operator : JC/MD Sample : J2649-01DL 20X Misc : 5.42g/5mL/100uL/5mL/MSVOA_X/MEOH ALS Vial : 7 Sample Multiplier: 1 Quant Time: May 11 07:46:14 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 247056 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 339982 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 298233 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 163647 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 193952 54.62 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.24% 35) Dibromofluoromethane 5.51 113 152029 50.27 ug/l 0.00 Spiked Amount 50.000 Recovery = 100.54% 50) Toluene-d8 8.72 98 546910 49.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 99.10% 62) 4-Bromofluorobenzene 11.14 95 179811 42.43 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.86% Target Compounds Qvalue 44) Trichloroethene 7.21 130 2539 0.66 ug/l 92 64) Tetrachloroethene 9.34 164 254676 61.27 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed