Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001603.D Acq On : 10 May 2018 15:53 Operator : JC/MD Sample : J2649-02DL 50X Misc : 6.13g/5mL/100uL/5mL/MSVOA_X/MEOH ALS Vial : 8 Sample Multiplier: 1 Quant Time: May 11 07:48:40 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 242483 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 329299 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 274875 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 135181 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 198796 57.04 ug/l 0.00 Spiked Amount 50.000 Recovery = 114.08% 35) Dibromofluoromethane 5.51 113 153700 52.47 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.94% 50) Toluene-d8 8.72 98 532405 49.80 ug/l 0.00 Spiked Amount 50.000 Recovery = 99.60% 62) 4-Bromofluorobenzene 11.14 95 165598 40.35 ug/l 0.00 Spiked Amount 50.000 Recovery = 80.70% Target Compounds Qvalue 64) Tetrachloroethene 9.34 164 128914 33.65 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed