Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001606.D Acq On : 10 May 2018 17:14 Operator : JC/MD Sample : J2738-03 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 11 Sample Multiplier: 1 Quant Time: May 11 07:39:09 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 234408 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 320513 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 276733 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 147874 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 196728 58.39 ug/l 0.00 Spiked Amount 50.000 Recovery = 116.78% 35) Dibromofluoromethane 5.51 113 154921 54.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.68% 50) Toluene-d8 8.72 98 535196 51.43 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.86% 62) 4-Bromofluorobenzene 11.15 95 175891 44.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.06% Target Compounds Qvalue 16) Acetone 2.45 43 6285 4.11 ug/l 98 18) Methyl Acetate 2.78 43 6534 1.63 ug/l 95 20) Methylene Chloride 2.86 84 44772 14.78 ug/l 99 95) Naphthalene 13.84 128 74867 6.83 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed