Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001607.D Acq On : 10 May 2018 17:40 Operator : JC/MD Sample : J2738-04 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 12 Sample Multiplier: 1 Quant Time: May 11 07:36:15 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 230545 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 313267 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 276644 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 150668 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 191399 57.76 ug/l 0.00 Spiked Amount 50.000 Recovery = 115.52% 35) Dibromofluoromethane 5.51 113 151476 54.36 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.72% 50) Toluene-d8 8.72 98 526566 51.77 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.54% 62) 4-Bromofluorobenzene 11.14 95 172948 44.29 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.58% Target Compounds Qvalue 16) Acetone 2.45 43 5967 3.97 ug/l 94 18) Methyl Acetate 2.79 43 6911 1.75 ug/l 100 20) Methylene Chloride 2.85 84 4775 1.60 ug/l 88 44) Trichloroethene 7.22 130 10181 2.86 ug/l 93 68) m/p-Xylenes 10.36 106 6132 1.17 ug/l 97 84) 1,2,4-Trimethylbenzene 11.81 105 24857 2.79 ug/l 99 95) Naphthalene 13.84 128 90435 8.10 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed