Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001608.D Acq On : 10 May 2018 18:07 Operator : JC/MD Sample : J2738-05 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 13 Sample Multiplier: 1 Quant Time: May 11 07:33:59 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 232983 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 313548 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 268455 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 136652 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.08 65 196383 58.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 117.28% 35) Dibromofluoromethane 5.51 113 153292 54.96 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.92% 50) Toluene-d8 8.72 98 534255 52.48 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.96% 62) 4-Bromofluorobenzene 11.14 95 172027 44.02 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.04% Target Compounds Qvalue 16) Acetone 2.45 43 7316 4.81 ug/l 89 18) Methyl Acetate 2.78 43 6923 1.73 ug/l 98 20) Methylene Chloride 2.86 84 54465 18.09 ug/l 97 44) Trichloroethene 7.22 130 56668 15.91 ug/l 100 68) m/p-Xylenes 10.36 106 22161 4.35 ug/l 98 69) o-Xylene 10.71 106 10872 2.19 ug/l 99 95) Naphthalene 13.84 128 255302 25.22 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed