Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001609.D Acq On : 10 May 2018 18:34 Operator : JC/MD Sample : J2738-02 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 14 Sample Multiplier: 1 Quant Time: May 11 07:31:06 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 233754 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 317199 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 270955 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 136162 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 195858 58.29 ug/l 0.00 Spiked Amount 50.000 Recovery = 116.58% 35) Dibromofluoromethane 5.51 113 151816 53.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.62% 50) Toluene-d8 8.72 98 525661 51.04 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.08% 62) 4-Bromofluorobenzene 11.15 95 167453 42.36 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.72% Target Compounds Qvalue 16) Acetone 2.45 43 9459 6.20 ug/l 100 18) Methyl Acetate 2.78 43 7723 1.93 ug/l 99 20) Methylene Chloride 2.86 84 3580 1.19 ug/l 93 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed