Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001610.D Acq On : 10 May 2018 19:01 Operator : JC/MD Sample : J1585-21 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 15 Sample Multiplier: 1 Quant Time: May 11 07:29:06 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 233641 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 317909 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 279496 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 149177 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 156158 46.50 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.00% 35) Dibromofluoromethane 5.51 113 123160 43.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.10% 50) Toluene-d8 8.72 98 432396 41.89 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.78% 62) 4-Bromofluorobenzene 11.14 95 139381 35.18 ug/l 0.00 Spiked Amount 50.000 Recovery = 70.36% Target Compounds Qvalue 16) Acetone 2.45 43 4932 3.23 ug/l 95 18) Methyl Acetate 2.78 43 8078 2.02 ug/l 100 20) Methylene Chloride 2.86 84 1329289 440.28 ug/l 98 95) Naphthalene 13.84 128 96535 8.74 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed