Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001611.D Acq On : 10 May 2018 19:28 Operator : JC/MD Sample : J1427-03 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 16 Sample Multiplier: 1 Quant Time: May 11 07:50:44 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 236297 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 318342 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 277956 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 148428 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 156246 46.00 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.00% 35) Dibromofluoromethane 5.51 113 123829 43.73 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.46% 50) Toluene-d8 8.72 98 430633 41.66 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.32% 62) 4-Bromofluorobenzene 11.14 95 139255 35.10 ug/l 0.00 Spiked Amount 50.000 Recovery = 70.20% Target Compounds Qvalue 16) Acetone 2.45 43 321667 208.58 ug/l 99 20) Methylene Chloride 2.86 84 5425 1.78 ug/l 97 25) 2-Butanone 4.72 43 12569 5.64 ug/l 95 30) Chloroform 5.23 83 53133 10.14 ug/l 98 52) Toluene 8.79 92 18652 2.41 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed