Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001612.D Acq On : 10 May 2018 19:55 Operator : JC/MD Sample : J2822-05 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 17 Sample Multiplier: 1 Quant Time: May 11 07:22:03 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 230062 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 309850 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 273917 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 147329 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 156338 47.28 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.56% 35) Dibromofluoromethane 5.51 113 121013 43.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.82% 50) Toluene-d8 8.72 98 425617 42.31 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.62% 62) 4-Bromofluorobenzene 11.14 95 136718 35.40 ug/l 0.00 Spiked Amount 50.000 Recovery = 70.80% Target Compounds Qvalue 7) Trichlorofluoromethane 1.93 101 5495 1.16 ug/l 100 16) Acetone 2.45 43 4225 2.81 ug/l 93 18) Methyl Acetate 2.79 43 9395 2.38 ug/l 95 64) Tetrachloroethene 9.34 164 43833 11.48 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed