Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001613.D Acq On : 10 May 2018 20:22 Operator : JC/MD Sample : J2836-06 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 18 Sample Multiplier: 1 Quant Time: May 11 07:52:02 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 234014 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 318662 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 284599 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 155344 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 159630 47.46 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.92% 35) Dibromofluoromethane 5.51 113 122566 43.24 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.48% 50) Toluene-d8 8.72 98 440684 42.59 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.18% 62) 4-Bromofluorobenzene 11.14 95 142243 35.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.62% Target Compounds Qvalue 16) Acetone 2.45 43 8764 5.74 ug/l 97 18) Methyl Acetate 2.79 43 6824 1.70 ug/l 98 20) Methylene Chloride 2.86 84 11772 3.89 ug/l 96 25) 2-Butanone 4.73 43 2557 1.16 ug/l 93 84) 1,2,4-Trimethylbenzene 11.81 105 10887 1.18 ug/l 98 95) Naphthalene 13.84 128 168185 14.62 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed