Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001614.D Acq On : 10 May 2018 20:48 Operator : JC/MD Sample : J2836-03 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 19 Sample Multiplier: 1 Quant Time: May 11 07:10:29 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 234634 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 317345 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 279110 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 146745 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.08 65 158669 47.05 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.10% 35) Dibromofluoromethane 5.51 113 122432 43.37 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.74% 50) Toluene-d8 8.72 98 437598 42.47 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.94% 62) 4-Bromofluorobenzene 11.15 95 138503 35.02 ug/l 0.00 Spiked Amount 50.000 Recovery = 70.04% Target Compounds Qvalue 16) Acetone 2.45 43 5742 3.75 ug/l 99 18) Methyl Acetate 2.78 43 6538 1.63 ug/l 92 20) Methylene Chloride 2.86 84 33642 11.10 ug/l 98 95) Naphthalene 13.84 128 41495 3.82 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed