Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051018\ Data File : VX001615.D Acq On : 10 May 2018 21:15 Operator : JC/MD Sample : J1585-11 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 20 Sample Multiplier: 1 Quant Time: May 11 07:08:47 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 231000 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 313635 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 272725 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 141927 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 158275 47.67 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.34% 35) Dibromofluoromethane 5.51 113 122875 44.05 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.10% 50) Toluene-d8 8.72 98 428138 42.04 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.08% 62) 4-Bromofluorobenzene 11.15 95 135211 34.59 ug/l 0.00 Spiked Amount 50.000 Recovery = 69.18% Target Compounds Qvalue 16) Acetone 2.45 43 4068 2.70 ug/l 96 18) Methyl Acetate 2.78 43 6411 1.62 ug/l 93 20) Methylene Chloride 2.86 84 7294 2.44 ug/l # 86 95) Naphthalene 13.84 128 51829 4.93 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed