Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001624.D Acq On : 11 May 2018 02:09 Operator : JC/MD Sample : VX0510WBL01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 31 Sample Multiplier: 1 Quant Time: May 11 07:32:56 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\624X051118W.M Quant Title : METHOD 624 VOLATILE ORGANIC ANALYSIS QLast Update : Fri May 11 07:16:13 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Bromochloromethane 5.03 128 54020 30.00 ug/l 0.00 28) 1,4-Difluorobenzene 6.87 114 281756 30.00 ug/l 0.00 57) Chlorobenzene-d5 10.12 117 245248 30.00 ug/l 0.00 System Monitoring Compounds 27) 1,2-Dichloroethane-d4 6.07 65 121441 30.81 ug/l 0.00 Spiked Amount 30.000 Range 50 - 169 Recovery = 102.70% 60) 4-Bromofluorobenzene 11.14 95 101384 26.12 ug/l 0.00 Spiked Amount 30.000 Range 56 - 143 Recovery = 87.07% 63) Toluene-d8 8.72 98 323585 29.59 ug/l 0.00 Spiked Amount 30.000 Range 66 - 137 Recovery = 98.63% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed