Quantitation Report    (QT Reviewed)

  Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\
  Data File : VX001628.D                                          
  Acq On    : 11 May 2018  03:55
  Operator  : JC/MD
  Sample    : J2766-02
  Misc      : 5.0mL/MSVOA_X/WATER
  ALS Vial  : 35   Sample Multiplier: 1

  Quant Time: May 11 07:45:45 2018
  Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\624X051118W.M
  Quant Title  : METHOD 624 VOLATILE ORGANIC ANALYSIS
  QLast Update : Fri May 11 07:16:13 2018
  Response via : Initial Calibration

   Internal Standards                R.T. QIon  Response  Conc Units Dev(Min)
   --------------------------------------------------------------------------
     1) Bromochloromethane           5.03  128    54778    30.00 ug/l    0.00
    28) 1,4-Difluorobenzene          6.87  114   286536    30.00 ug/l    0.00
    57) Chlorobenzene-d5            10.12  117   252890    30.00 ug/l    0.00

   System Monitoring Compounds                                        
    27) 1,2-Dichloroethane-d4        6.07   65   120832    30.23 ug/l    0.00  
     Spiked Amount     30.000   Range  50 - 169    Recovery   =  100.77% 
    60) 4-Bromofluorobenzene        11.14   95   118022    29.49 ug/l    0.00  
     Spiked Amount     30.000   Range  56 - 143    Recovery   =   98.30% 
    63) Toluene-d8                   8.72   98   334406    29.65 ug/l    0.00  
     Spiked Amount     30.000   Range  66 - 137    Recovery   =   98.83% 

   Target Compounds                                                   Qvalue
    15) Acetone                      2.45   58  1098709  2374.96 ug/l      93
    16) Carbon Disulfide             2.57   76     9684     1.54 ug/l     100
    30) 2-Butanone                   4.72   43    54686    23.02 ug/l     100
    58) 4-Methyl-2-Pentanone         8.66   43    15013     3.30 ug/l      97
    61) Tetrachloroethene            9.34  164     7669     2.08 ug/l      96
    62) Toluene                      8.79   91    42046     3.46 ug/l      98
    66) Ethyl Benzene               10.26   91     5133     0.41 ug/l      96
    67) m/p-Xylenes                 10.36  106     2401     0.48 ug/l      99
    68) o-Xylene                    10.71  106     1159     0.23 ug/l      97
    69) Styrene                     10.72  104     2699     0.33 ug/l      98
    79) tert-butylbenzene           12.07  119   240829    21.05 ug/l      99
    80) 1,2,4-Trimethylbenzene      11.82  105    17022     1.54 ug/l      54
    81) sec-Butylbenzene            11.95  105     7157m    0.57 ug/l        
    82) p-Isopropyltoluene          12.07  119   240829    21.05 ug/l      99
    91) Naphthalene                 13.84  128     7542     0.50 ug/l #    94
   --------------------------------------------------------------------------

   (#) = qualifier out of range (m) = manual integration (+) = signals summed