Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001631.D Acq On : 11 May 2018 09:52 Operator : JC/MD Sample : J2801-01DL 20X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 38 Sample Multiplier: 1 Quant Time: May 11 12:24:28 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\624X051118W.M Quant Title : METHOD 624 VOLATILE ORGANIC ANALYSIS QLast Update : Fri May 11 07:16:13 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Bromochloromethane 5.02 128 49393 30.00 ug/l 0.00 28) 1,4-Difluorobenzene 6.87 114 282585 30.00 ug/l 0.00 57) Chlorobenzene-d5 10.12 117 254866 30.00 ug/l 0.00 System Monitoring Compounds 27) 1,2-Dichloroethane-d4 6.07 65 115925 32.17 ug/l 0.00 Spiked Amount 30.000 Range 50 - 169 Recovery = 107.23% 60) 4-Bromofluorobenzene 11.15 95 122899 30.47 ug/l 0.00 Spiked Amount 30.000 Range 56 - 143 Recovery = 101.57% 63) Toluene-d8 8.72 98 329064 28.95 ug/l 0.00 Spiked Amount 30.000 Range 66 - 137 Recovery = 96.50% Target Compounds Qvalue 15) Acetone 2.47 58 37703 90.38 ug/l 95 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed