Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001632.D Acq On : 11 May 2018 10:18 Operator : JC/MD Sample : J2801-02DL 100X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 39 Sample Multiplier: 1 Quant Time: May 11 10:48:34 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\624X051118W.M Quant Title : METHOD 624 VOLATILE ORGANIC ANALYSIS QLast Update : Fri May 11 07:16:13 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Bromochloromethane 5.03 128 54935 30.00 ug/l 0.00 28) 1,4-Difluorobenzene 6.87 114 293691 30.00 ug/l 0.00 57) Chlorobenzene-d5 10.12 117 255158 30.00 ug/l 0.00 System Monitoring Compounds 27) 1,2-Dichloroethane-d4 6.07 65 122301 30.51 ug/l 0.00 Spiked Amount 30.000 Range 50 - 169 Recovery = 101.70% 60) 4-Bromofluorobenzene 11.14 95 109127 27.02 ug/l 0.00 Spiked Amount 30.000 Range 56 - 143 Recovery = 90.07% 63) Toluene-d8 8.72 98 332793 29.25 ug/l 0.00 Spiked Amount 30.000 Range 66 - 137 Recovery = 97.50% Target Compounds Qvalue 15) Acetone 2.45 58 37342 80.49 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed