Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001641.D Acq On : 11 May 2018 16:07 Operator : JC/MD Sample : J2741-01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 7 Sample Multiplier: 1 Quant Time: May 12 12:08:06 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 254793 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 347349 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 304785 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 163527 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 199358 54.44 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.88% 35) Dibromofluoromethane 5.51 113 159514 51.63 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.26% 50) Toluene-d8 8.72 98 560159 49.67 ug/l 0.00 Spiked Amount 50.000 Recovery = 99.34% 62) 4-Bromofluorobenzene 11.15 95 184175 42.54 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.08% Target Compounds Qvalue 21) trans-1,2-Dichloroethene 3.17 96 2317 0.74 ug/l 94 27) cis-1,2-Dichloroethene 4.60 96 290635 86.73 ug/l 86 44) Trichloroethene 7.22 130 99618 25.25 ug/l 99 64) Tetrachloroethene 9.34 164 1017520 239.51 ug/l 100 65) Chlorobenzene 10.14 112 3396 0.38 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed