Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001642.D Acq On : 11 May 2018 16:34 Operator : JC/MD Sample : J2741-02 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 8 Sample Multiplier: 1 Quant Time: May 12 06:58:32 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 252091 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 336999 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 287539 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 147921 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 202545 55.90 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.80% 35) Dibromofluoromethane 5.51 113 161466 53.87 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.74% 50) Toluene-d8 8.72 98 570467 52.14 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.28% 62) 4-Bromofluorobenzene 11.15 95 181659 43.25 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.50% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 12648 3.67 ug/l 97 12) 1,1-Dichloroethene 2.38 96 1072 0.38 ug/l 91 21) trans-1,2-Dichloroethene 3.17 96 3349 1.08 ug/l 92 27) cis-1,2-Dichloroethene 4.60 96 649982 196.05 ug/l 86 44) Trichloroethene 7.22 130 129127 33.74 ug/l 100 64) Tetrachloroethene 9.34 164 281317 70.19 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed