Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001643.D Acq On : 11 May 2018 17:01 Operator : JC/MD Sample : J2741-03 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 9 Sample Multiplier: 1 Quant Time: May 12 07:00:57 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 256733 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 343991 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 299733 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 161703 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 207539 56.24 ug/l 0.00 Spiked Amount 50.000 Recovery = 112.48% 35) Dibromofluoromethane 5.51 113 165254 54.01 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.02% 50) Toluene-d8 8.72 98 581875 52.10 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.20% 62) 4-Bromofluorobenzene 11.15 95 190419 44.41 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.82% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 35615 10.14 ug/l 95 12) 1,1-Dichloroethene 2.38 96 1992 0.70 ug/l # 87 21) trans-1,2-Dichloroethene 3.17 96 1918 0.60 ug/l # 81 27) cis-1,2-Dichloroethene 4.60 96 320326 94.87 ug/l 87 44) Trichloroethene 7.22 130 20602 5.27 ug/l 99 64) Tetrachloroethene 9.34 164 18267 4.37 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed