Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001644.D Acq On : 11 May 2018 17:27 Operator : JC/MD Sample : J2741-04 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 10 Sample Multiplier: 1 Quant Time: May 12 07:02:57 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 244372 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 336376 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 287695 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 155362 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.08 65 201344 57.32 ug/l 0.00 Spiked Amount 50.000 Recovery = 114.64% 35) Dibromofluoromethane 5.51 113 157967 52.80 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.60% 50) Toluene-d8 8.72 98 556107 50.92 ug/l 0.00 Spiked Amount 50.000 Recovery = 101.84% 62) 4-Bromofluorobenzene 11.15 95 184169 43.93 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.86% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 95007 29.56 ug/l 86 44) Trichloroethene 7.22 130 5608 1.47 ug/l 96 64) Tetrachloroethene 9.34 164 4586 1.14 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed