Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001645.D Acq On : 11 May 2018 17:54 Operator : JC/MD Sample : J2741-05 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 11 Sample Multiplier: 1 Quant Time: May 12 07:05:08 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 248315 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 332187 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 288756 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 148644 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 194115 54.39 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.78% 35) Dibromofluoromethane 5.51 113 154957 52.44 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.88% 50) Toluene-d8 8.72 98 541435 50.20 ug/l 0.00 Spiked Amount 50.000 Recovery = 100.40% 62) 4-Bromofluorobenzene 11.14 95 173462 41.90 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.80% Target Compounds Qvalue 9) 1,1,2-Trichlorotrifluoroet 2.39 101 27024 9.01 ug/l 97 12) 1,1-Dichloroethene 2.38 96 862 0.31 ug/l 84 21) trans-1,2-Dichloroethene 3.17 96 1408 0.46 ug/l 93 27) cis-1,2-Dichloroethene 4.60 96 435651 133.40 ug/l 86 44) Trichloroethene 7.22 130 70472 18.68 ug/l 94 64) Tetrachloroethene 9.34 164 625740 155.47 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed