Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001646.D Acq On : 11 May 2018 18:21 Operator : JC/MD Sample : J2741-06 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 12 Sample Multiplier: 1 Quant Time: May 12 07:06:34 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 242738 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 331157 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 291739 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 158511 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 199622 57.22 ug/l 0.00 Spiked Amount 50.000 Recovery = 114.44% 35) Dibromofluoromethane 5.51 113 158659 53.86 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.72% 50) Toluene-d8 8.72 98 557038 51.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.62% 62) 4-Bromofluorobenzene 11.15 95 184159 44.62 ug/l 0.00 Spiked Amount 50.000 Recovery = 89.24% Target Compounds Qvalue 21) trans-1,2-Dichloroethene 3.17 96 2353 0.78 ug/l 93 27) cis-1,2-Dichloroethene 4.60 96 279255 87.47 ug/l 87 44) Trichloroethene 7.22 130 95475 25.39 ug/l 100 64) Tetrachloroethene 9.34 164 1013923 249.34 ug/l 99 65) Chlorobenzene 10.15 112 4077 0.48 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed