Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001647.D Acq On : 11 May 2018 18:48 Operator : JC/MD Sample : J2741-07 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 13 Sample Multiplier: 1 Quant Time: May 12 07:08:13 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 252624 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 337455 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 294475 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 157377 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 203066 55.93 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.86% 35) Dibromofluoromethane 5.51 113 163022 54.31 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.62% 50) Toluene-d8 8.72 98 566328 51.69 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.38% 62) 4-Bromofluorobenzene 11.14 95 184891 43.96 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.92% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 252369 73.01 ug/l 99 12) 1,1-Dichloroethene 2.37 96 5680 2.03 ug/l 95 21) trans-1,2-Dichloroethene 3.17 96 5824 1.87 ug/l 99 24) 1,1-Dichloroethane 3.70 63 9002 1.65 ug/l 99 27) cis-1,2-Dichloroethene 4.60 96 2607942 784.94 ug/l 85 44) Trichloroethene 7.22 130 4116 1.07 ug/l 99 64) Tetrachloroethene 9.34 164 8024 1.95 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed