Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001648.D Acq On : 11 May 2018 19:15 Operator : JC/MD Sample : J2741-10 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 14 Sample Multiplier: 1 Quant Time: May 12 07:13:07 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 243301 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 327722 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 287506 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 153615 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 199386 57.02 ug/l 0.00 Spiked Amount 50.000 Recovery = 114.04% 35) Dibromofluoromethane 5.51 113 157858 54.15 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.30% 50) Toluene-d8 8.72 98 551315 51.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.62% 62) 4-Bromofluorobenzene 11.14 95 180781 44.26 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.52% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 926 0.28 ug/l # 75 21) trans-1,2-Dichloroethene 3.17 96 2994 1.00 ug/l # 90 27) cis-1,2-Dichloroethene 4.60 96 175895 54.97 ug/l 86 44) Trichloroethene 7.22 130 72781 19.56 ug/l 99 64) Tetrachloroethene 9.34 164 803664 200.54 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed