Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001649.D Acq On : 11 May 2018 19:41 Operator : JC/MD Sample : J2741-11 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 15 Sample Multiplier: 1 Quant Time: May 12 07:14:15 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 235814 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 320714 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 283636 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 149591 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.08 65 197107 58.15 ug/l 0.00 Spiked Amount 50.000 Recovery = 116.30% 35) Dibromofluoromethane 5.51 113 156693 54.93 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.86% 50) Toluene-d8 8.72 98 544673 52.31 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.62% 62) 4-Bromofluorobenzene 11.15 95 178064 44.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 89.10% Target Compounds Qvalue 21) trans-1,2-Dichloroethene 3.17 96 2840 0.98 ug/l 94 27) cis-1,2-Dichloroethene 4.60 96 124071 40.00 ug/l 86 44) Trichloroethene 7.22 130 61809 16.97 ug/l 97 64) Tetrachloroethene 9.34 164 783566 198.20 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed