Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001650.D Acq On : 11 May 2018 20:08 Operator : JC/MD Sample : J2741-13 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 16 Sample Multiplier: 1 Quant Time: May 12 07:17:17 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 235080 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 316187 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 270525 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 132733 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 195162 57.76 ug/l 0.00 Spiked Amount 50.000 Recovery = 115.52% 35) Dibromofluoromethane 5.51 113 155697 55.36 ug/l 0.00 Spiked Amount 50.000 Recovery = 110.72% 50) Toluene-d8 8.72 98 531377 51.76 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.52% 62) 4-Bromofluorobenzene 11.14 95 165215 41.92 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.84% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 7257 2.26 ug/l # 68 27) cis-1,2-Dichloroethene 4.60 96 22584 7.30 ug/l 90 44) Trichloroethene 7.22 130 3117 0.87 ug/l 83 64) Tetrachloroethene 9.34 164 13792 3.66 ug/l 94 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed