Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001652.D Acq On : 11 May 2018 21:02 Operator : JC/MD Sample : J2741-15 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 18 Sample Multiplier: 1 Quant Time: May 12 07:22:06 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 248155 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 332631 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 297121 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 158410 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 200128 56.11 ug/l 0.00 Spiked Amount 50.000 Recovery = 112.22% 35) Dibromofluoromethane 5.51 113 159821 54.02 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.04% 50) Toluene-d8 8.72 98 556172 51.50 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.00% 62) 4-Bromofluorobenzene 11.14 95 182940 44.13 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.26% Target Compounds Qvalue 21) trans-1,2-Dichloroethene 3.17 96 2175 0.71 ug/l 84 27) cis-1,2-Dichloroethene 4.60 96 126480 38.75 ug/l 86 30) Chloroform 5.23 83 3265 0.59 ug/l 98 44) Trichloroethene 7.22 130 64664 17.12 ug/l 95 64) Tetrachloroethene 9.34 164 461492 111.43 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed