Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001653.D Acq On : 11 May 2018 21:28 Operator : JC/MD Sample : J2741-16 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 19 Sample Multiplier: 1 Quant Time: May 12 07:24:16 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 239497 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 324707 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 283773 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 150547 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 240296 69.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 139.62% 35) Dibromofluoromethane 5.51 113 191229 66.21 ug/l 0.00 Spiked Amount 50.000 Recovery = 132.42% 50) Toluene-d8 8.72 98 663853 62.97 ug/l 0.00 Spiked Amount 50.000 Recovery = 125.94% 62) 4-Bromofluorobenzene 11.14 95 216985 53.62 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.24% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 14734 4.68 ug/l 96 30) Chloroform 5.23 83 2081 0.39 ug/l 98 44) Trichloroethene 7.22 130 9631 2.61 ug/l 97 64) Tetrachloroethene 9.34 164 46567 11.77 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed