Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051118\ Data File : VX001654.D Acq On : 11 May 2018 21:55 Operator : JC/MD Sample : J2741-17 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 20 Sample Multiplier: 1 Quant Time: May 12 07:26:00 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 241601 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 328310 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 284744 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 148713 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 203955 58.73 ug/l 0.00 Spiked Amount 50.000 Recovery = 117.46% 35) Dibromofluoromethane 5.51 113 159777 54.71 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.42% 50) Toluene-d8 8.72 98 558101 52.36 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.72% 62) 4-Bromofluorobenzene 11.14 95 178139 43.53 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.06% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 11673 3.67 ug/l 93 44) Trichloroethene 7.22 130 4091 1.10 ug/l 97 64) Tetrachloroethene 9.34 164 34311 8.64 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed