Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001662.D Acq On : 12 May 2018 13:09 Operator : JC/MD Sample : J2741-18 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 5 Sample Multiplier: 1 Quant Time: May 14 06:41:40 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 269541 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 362544 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 303425 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 151152 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 216812 55.96 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.92% 35) Dibromofluoromethane 5.51 113 172675 53.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.10% 50) Toluene-d8 8.72 98 608630 51.71 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.42% 62) 4-Bromofluorobenzene 11.14 95 186738 41.33 ug/l 0.00 Spiked Amount 50.000 Recovery = 82.66% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 25392 7.16 ug/l 91 30) Chloroform 5.23 83 2692 0.45 ug/l 94 44) Trichloroethene 7.22 130 7255 1.76 ug/l 85 64) Tetrachloroethene 9.34 164 31488 7.45 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed