Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001663.D Acq On : 12 May 2018 13:36 Operator : JC/MD Sample : J2741-19 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 6 Sample Multiplier: 1 Quant Time: May 14 06:44:02 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 276135 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 370770 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 327682 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 176838 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 220273 55.50 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.00% 35) Dibromofluoromethane 5.51 113 175963 53.36 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.72% 50) Toluene-d8 8.72 98 626301 52.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.06% 62) 4-Bromofluorobenzene 11.14 95 206316 44.65 ug/l 0.00 Spiked Amount 50.000 Recovery = 89.30% Target Compounds Qvalue 21) trans-1,2-Dichloroethene 3.17 96 2221 0.65 ug/l 88 27) cis-1,2-Dichloroethene 4.60 96 685991 188.89 ug/l 85 44) Trichloroethene 7.22 130 54596 12.97 ug/l 99 64) Tetrachloroethene 9.34 164 1277031 279.60 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed