Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001665.D Acq On : 12 May 2018 14:29 Operator : JC/MD Sample : J2741-16 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 8 Sample Multiplier: 1 Quant Time: May 14 06:52:27 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 265912 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 358699 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 312365 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 165426 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 215426 56.36 ug/l 0.00 Spiked Amount 50.000 Recovery = 112.72% 35) Dibromofluoromethane 5.51 113 172619 54.10 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.20% 50) Toluene-d8 8.72 98 604214 51.88 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.76% 62) 4-Bromofluorobenzene 11.15 95 194291 43.46 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.92% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 14678 4.20 ug/l 95 30) Chloroform 5.21 83 2167 0.37 ug/l # 80 44) Trichloroethene 7.22 130 9890 2.43 ug/l 91 64) Tetrachloroethene 9.34 164 49015 11.26 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed