Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001667.D Acq On : 12 May 2018 15:23 Operator : JC/MD Sample : J2741-01DL 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 10 Sample Multiplier: 1 Quant Time: May 14 07:11:31 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 268914 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 363434 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 315396 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 169178 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 212849 55.07 ug/l 0.00 Spiked Amount 50.000 Recovery = 110.14% 35) Dibromofluoromethane 5.51 113 171645 53.10 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.20% 50) Toluene-d8 8.72 98 607364 51.47 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.94% 62) 4-Bromofluorobenzene 11.14 95 195965 43.26 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.52% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 52557 14.86 ug/l 87 44) Trichloroethene 7.22 130 17972 4.35 ug/l 100 64) Tetrachloroethene 9.34 164 159429 36.27 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed