Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001668.D Acq On : 12 May 2018 15:49 Operator : JC/MD Sample : J2741-02DL 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 11 Sample Multiplier: 1 Quant Time: May 14 07:12:43 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 268716 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 360080 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 312230 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 167564 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 214242 55.47 ug/l 0.00 Spiked Amount 50.000 Recovery = 110.94% 35) Dibromofluoromethane 5.51 113 171822 53.65 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.30% 50) Toluene-d8 8.72 98 598510 51.19 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.38% 62) 4-Bromofluorobenzene 11.14 95 191346 42.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.28% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 2635 0.72 ug/l 96 27) cis-1,2-Dichloroethene 4.60 96 123446 34.93 ug/l 87 44) Trichloroethene 7.22 130 24544 6.00 ug/l 98 64) Tetrachloroethene 9.34 164 53098 12.20 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed