Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001669.D Acq On : 12 May 2018 16:16 Operator : JC/MD Sample : J2741-05DL 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 12 Sample Multiplier: 1 Quant Time: May 14 07:13:44 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 260296 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 348505 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 298478 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 155898 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 208264 55.67 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.34% 35) Dibromofluoromethane 5.51 113 165472 53.38 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.76% 50) Toluene-d8 8.72 98 574435 50.77 ug/l 0.00 Spiked Amount 50.000 Recovery = 101.54% 62) 4-Bromofluorobenzene 11.14 95 182031 41.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.82% Target Compounds Qvalue 9) 1,1,2-Trichlorotrifluoroet 2.39 101 4471 1.42 ug/l 98 27) cis-1,2-Dichloroethene 4.60 96 76761 22.42 ug/l 86 44) Trichloroethene 7.22 130 12536 3.17 ug/l 100 64) Tetrachloroethene 9.34 164 101715 24.45 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed