Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001671.D Acq On : 12 May 2018 17:09 Operator : JC/MD Sample : J2741-07DL 10X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 14 Sample Multiplier: 1 Quant Time: May 14 07:15:59 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 264863 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 356360 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 310379 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 165507 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 211831 55.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.28% 35) Dibromofluoromethane 5.51 113 169629 53.51 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.02% 50) Toluene-d8 8.72 98 591865 51.15 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.30% 62) 4-Bromofluorobenzene 11.14 95 191137 43.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.06% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 25620 7.07 ug/l 98 27) cis-1,2-Dichloroethene 4.60 96 254565 73.08 ug/l 86 64) Tetrachloroethene 9.34 164 1473 0.34 ug/l 89 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed