Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001673.D Acq On : 12 May 2018 18:03 Operator : JC/MD Sample : J2741-11DL 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 16 Sample Multiplier: 1 Quant Time: May 14 07:18:07 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 260013 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 352082 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 307233 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 162871 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 211151 56.50 ug/l 0.00 Spiked Amount 50.000 Recovery = 113.00% 35) Dibromofluoromethane 5.51 113 168258 53.73 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.46% 50) Toluene-d8 8.72 98 592063 51.79 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.58% 62) 4-Bromofluorobenzene 11.14 95 190724 43.46 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.92% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 25928 7.58 ug/l 88 44) Trichloroethene 7.22 130 13290 3.32 ug/l 100 64) Tetrachloroethene 9.34 164 164209 38.35 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed