Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001674.D Acq On : 12 May 2018 18:29 Operator : JC/MD Sample : J2741-19DL 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 17 Sample Multiplier: 1 Quant Time: May 14 07:18:59 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 264056 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 352989 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 314632 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 167167 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 173130 45.62 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.24% 35) Dibromofluoromethane 5.51 113 137331 43.74 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.48% 50) Toluene-d8 8.72 98 485505 42.36 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.72% 62) 4-Bromofluorobenzene 11.14 95 157518 35.80 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.60% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 127002 36.57 ug/l 86 44) Trichloroethene 7.22 130 10018 2.50 ug/l 93 64) Tetrachloroethene 9.34 164 230442 52.55 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed