Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001675.D Acq On : 12 May 2018 18:56 Operator : JC/MD Sample : J2741-18 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 18 Sample Multiplier: 1 Quant Time: May 14 07:20:15 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 258859 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 352697 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 304117 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 159375 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 209948 56.43 ug/l 0.00 Spiked Amount 50.000 Recovery = 112.86% 35) Dibromofluoromethane 5.51 113 167508 53.39 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.78% 50) Toluene-d8 8.72 98 590825 51.59 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.18% 62) 4-Bromofluorobenzene 11.14 95 186665 42.46 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.92% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 24315 7.14 ug/l 89 30) Chloroform 5.22 83 2529 0.44 ug/l 88 44) Trichloroethene 7.22 130 6840 1.71 ug/l 97 47) Bromodichloromethane 7.91 83 1068 0.25 ug/l # 87 64) Tetrachloroethene 9.34 164 31138 7.35 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed